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GRC NMR Core Facility

GRC_400_turn_2

Enter GRC NMR Reservation System

GRC NMR Operation Guidelines
User's Account Application form[1]
GRC-NMR-Reservation form[2]
GRC-NMR-Reservation form[3]


AV400_GRC (400MHz NMR Spectrometer)

The AV400_GRC is located on the 19th floor of Incubation Center in Nankang Software Park. This NMR spectrometer is equipped with a high performance actively shielded standard bore 9.40 Tesla superconducting magnet (horizontal 5G line from magnetic centre less than 0.5m). The console has two channels, and the system is equipped with a regular 5mm 1H/13C dual probehead. The probehead includes Z-gradient and automated tuning/matching functions. This instrument could carry out 1H and 13C spectra as routine service.

5mm 1H/13C Dual-Z probehead
1H Sensitivity (0.1%EB in CDCL3) ~ 282:1
13C Sensitivity (10% EB in CDCL3) ~ 193:1
Temperature Range: 25oC ~ 80oC
Auto Tune and Match

GRC_600_s

 

AV600_GRC (600MHz NMR Spectrometer)

The AV600_GRC is located on the first floor of Genomics Research Center. This high field NMR spectrometer is equipped with a high performance actively shielded standard bore 14.09 Tesla superconducting magnet (horizontal 5G line from magnetic centre less than 0.7m). The console has two channels and two probeheads could be selected : regular 5mm BBO-Z (broadband observe for 31P to 15N and 1H decoupling, with Z-gradient and automated tuning/matching), and 5mm DCI Dual cryoprobe (high sensitivity 1H/13C observation includes cooled preamplifiers for 1H/13C/2H with Z-gradient) with CryoFit accessory (flow insert for LC-NMR application). The LC system consists of an Agilent Quaternary Chromatography System and Bruker LC-NMR accessory including on-flow, stop-flow, column switch, extended loop sampling, and solid phase extraction options. In addition to routine NMR service, the system could be used for high efficient LC-NMR application.

5mm BBO-Z probehead
1H Sensitivity (0.1%EB in CDCL3) ~ 490:1
13C Sensitivity (10% EB in CDCL3) ~ 296:1
15N Sensitivity (90% Formamide in DMSO) ~ 49:1
31P Sensitivity (0.0485M TPP in Acetone-d6) ~ 182:1
Temperature Range: 0oC ~ 80oC
Auto Tune and Match

5mm Cryoprobe DCI 1H/13C –Z probehead
1H Sensitivity (0.1%EB in CDCL3) ~ 3956:1
13C Sensitivity (10% EB in CDCL3) ~ 1513:1
Temperature Range: 0oC ~ 60oC

LC Interface
CryoFit 30ul Flow Cell
Aglient 1100 Quaternary Chromatography
On-Flow and Stop-Flow Measurement
36 Loops Sampling Unit
192 Cartridges Solid Phase Extraction